ࡱ> AC>?@q`  bjbjqPqP 4t:: ppp8Tpp uuuuuuuu$h)huuuuuuuővvvuuuvuvvvuu Ihpudvvۑ0 vvdvv,uuvuuuuuvRuuu uuuuDkpp Table S1. Atomic displacement parameters for holtite. H1H2H3H4Al(1)U110.0353(2)0.0352(2)0.0101(2)0.066(2)U220.0050(1)0.0050(1)0.0020(2)0.007(2)U330.0058(1)0.0058(1)0.0031(2)0.018(2)U120000U130.00260(8)0.0027(1)0.0001(1)0.004(2)U230000Al(2)U110.0042(2)0.0047(2)0.0030(3)0.013(2)U220.0059(2)0.0055(2)0.0035(3)0.007(2)U330.0060(2)0.0056(2)0.0051(3)0.015(2)U120.0000(1)0.0002(2)0.0004(2)0.003(1)U130.0002(1)0.0001(2)0.0004(2)0.001(1)U230.0001(1)0.0002(2)0.0001(2)0.001(1)Al(3)U110.0039(2)0.0040(2)0.0033(3)0.009(2)U220.0066(2)0.0058(2)0.0044(3)0.010(2)U330.0056(2)0.0049(2)0.0045(3)0.013(2)U120.0001(1)0.0000(2)0.0004(2)0.003(1)U130.0000(1)0.0001(1)0.0000(2)0.003(1)U230.0000(1)0.0000(1)0.0002(2)0.000(1)Al(4)U110.0070(2)0.0071(2)0.0063(3)0.014(2)U220.0089(2)0.0078(2)0.0054(3)0.009(2)U330.0079(2)0.0070(2)0.0065(3)0.014(2)U120.0002(2)0.0001(2)0.0001(2)0.000(1)U130.0004(1)0.0006(2)0.0011(2)0.002(2)U230.0013(2)0.0012(2)0.0007(2)0.000(1)Si(1)U110.0037(4)0.0036(4)0.0020(6)0.008(5)U220.0050(3)0.0048(3)0.0027(5)0.014(5)U330.0076(5)0.0065(6)0.0051(7)0.031(6)U120000U130.0001(4)0.0001(5)0.0000(7)0.001(5)U230000Sb1U110.0049(8)0.005(1)0.0044(4)0.010(4)U220.0071(7)0.0051(8)0.0039(4)0.005(3)U330.020(2)0.021(2)0.0120(7)0.032(4)U120000U130.0023(9)0.001(1)0.0009(5)0.005(3)U230000Si(2)U110.0043(2)0.0048(3)0.0031(4)0.011(3)U220.0070(3)0.0069(4)0.0048(5)0.009(4)U330.0052(3)0.0044(3)0.0045(4)0.008(4)U120.0005(2)0.0005(3)0.0004(4)0.004(2)U130.0001(2)0.0003(2)0.0006(3)0.004(2)U230.0005(2)0.0003(2)0.0002(4)0.002(2)Sb(2)U110.0062(4)0.0062(6)0.0046(3)0.015(2)U220.0132(9)0.015(1)0.0076(5)0.015(3)U330.0073(6)0.0065(8)0.0057(3)0.015(3)U120.0012(4)0.0013(6)0.0000(3)0.000(2)U130.0001(3)0.0018(4)0.0006(2)0.001(2)U230.0024(5)0.0033(7)0.0012(3)0.001(2)BU110.0056(8)0.006(1)0.002(1)0.034(7)U220.0079(8)0.007(1)0.005(1)0.011(7)U330.0075(8)0.006(1)0.007(1)0.006(7)U120000U130.0006(7)0.0006(8)0.001(1)0.004(7)U230000O(1)U110.0055(6)0.0057(6)0.0056(9)0.008(5)U220.0063(6)0.0057(6)0.0038(8)0.009(4)U330.0097(6)0.0076(7)0.0078(9)0.021(5)U120000U130.0010(5)0.0008(5)0.0004(7)0.004(4)U230000O(2)U110.0130(8)0.0134(9)0.014(1)0.011(6)U220.0108(8)0.0107(8)0.009(1)0.024(8)U330.0073(8)0.0076(9)0.003(1)0.033(4)U120000U130.0028(6)0.0016(6)0.001(1)0.006(5)U230000O(3)U110.0052(4)0.0046(5)0.0026(6)0.014(4)U220.0067(4)0.0062(5)0.0044(6)0.006(4)U330.0087(4)0.0080(5)0.0096(6)0.019(4)U120.0002(3)0.0003(4)0.0002(5)0.005(3)U130.0006(3)0.0003(4)0.0002(5)0.003(3)U230.0011(3)0.0007(3)0.0002(5)0.009(3)O(4)U110.0070(4)0.0066(5)0.0043(6)0.010(4)U220.0091(4)0.0080(5)0.0060(6)0.013(4)U330.0085(4)0.0074(5)0.0085(6)0.013(4)U120.0003(3)0.0004(4)0.0002(5)0.001(3)U130.0000(3)0.0003(4)0.0005(5)0.001(3)U230.0018(3)0.0014(4)0.0014(5)0.001(3)O(5)U110.0055(4)0.0056(5)0.0035(6)0.008(3)U220.0091(4)0.0082(5)0.0062(6)0.007(3)U330.0061(4)0.0050(5)0.0052(6)0.015(3)U120.0010(3)0.0006(4)0.0000(5)0.000(3)U130.0004(3)0.0001(3)0.0007(5)0.001(3)U230.0002(3)0.0001(4)0.0003(5)0.003(3)O(6)U110.0071(4)0.0070(5)0.0053(6)0.013(3)U220.0093(4)0.0075(5)0.0059(6)0.016(4)U330.0070(4)0.0064(5)0.0066(6)0.011(4)U120.0011(3)0.0008(4)0.0010(5)0.001(3)U130.0016(3)0.0015(4)0.0010(5)0.005(3)U230.0012(3)0.0008(4)0.0007(5)0.005(3)O(7)U110.0122(6)0.0128(6)0.009(1)0.020(5)U220.0109(6)0.0102(7)0.008(1)0.016(5)U330.0118(6)0.0095(6)0.009(1)0.030(6)U120.0010(4)0.0021(4)0.0011(8)0.002(4)U130.0009(4)0.0007(4)0.0018(8)0.010(4)U230.0018(4)0.0007(5)0.0020(8)0.004(3)O(8)U110.0158(7)0.0138(7)0.011(1)0.030(6)U220.0072(6)0.0058(7)0.0050(9)0.003(6)U330.0070(6)0.0067(7)0.0054(9)0.004(5)U120000U130.0018(5)0.0016(5)0.0023(8)0.001(5)U230000O(9)U110.0085(4)0.0082(5)0.0066(7)0.018(4)U220.0062(4)0.0060(4)0.0035(6)0.014(5)U330.0075(4)0.0064(5)0.0071(6)0.021(5)U120.0005(3)0.0005(4)0.0004(5)0.000(3)U130.0014(3)0.0015(4)0.0009(5)0.002(3)U230.0009(3)0.0002(4)0.0005(5)0.003(3)O(10)U110.0085(6)0.0086(7)0.0039(9)0.018(9)U220.0111(6)0.0098(7)0.0071(9)0.010(7)U330.0132(7)0.0124(7)0.0130(9)0.015(7)U120000U130.0003(5)0.0007(6)0.0000(8)0.005(5)U230000O(11)U110.0037(4)0.0042(4)0.0023(6)0.001(4)U220.0064(4)0.0067(5)0.0043(6)0.012(5)U330.0060(4)0.0047(4)0.0044(6)0.009(5)U120.0005(3)0.0003(4)0.0003(5)0.002(3)U130.0001(3)0.0001(3)0.0006(4)0.002(3)U230.0001(3)0.0001(3)0.0003(5)0.006(3)     4568DFGHIJKLOPcdmnvxy|}     ȹȹȹȹȹȹȹȹȹȹȹȹȹ&hAD$dd$G$Ifa$gd G H P R S V W j k t u }     ŶŶŶŶŶŶŶŶŶŶŶŶŶŶŶŶŶ&h ? @ A B E F Y Z c d l n o r s       # % & ) * = ȼȼȼȼȼȠ&h G H P S T U V W X [ \ o p y z        ' ) 2 4 < > ? 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